CEE 772 |
Fall 2019 |
Click on L# to see full Overheads or P# to see printable version (2 slides/pg)
Date |
Day |
L# |
P# |
Lecture |
Assignments |
|
Notes |
4 Sept |
W |
I. Introduction·
Course overview, administration, chemistry review
|
S:pp.1-11 H:Chapt. 0 |
|
|||
9 Sept |
M |
·
Basics of Instrumental Analysis
· Statistics |
|
S: pp.11-18 H: Chapt
1-4 |
|
||
10 Sept |
Tu |
·
Detection
Limits II. Spectroscopy·
Electron
Transitions ·
Beer-Lambert’s
Law |
|
S: pp.116-120, 134-140,
300-312 H:Chapt.
1 |
Class instead of lab today |
||
11 Sept 16 Sept |
W M |
A. Molecular Spec.·
UV-Vis ·
Properties of spectrophotometers ·
Wavelength
selectors |
S: Chapt.
14 H:Chapt.
19 |
Class instead of lab today |
|||
17 Sept |
Tu |
|
ISB Chem lab |
||||
18 Sept 23 Sept |
W M |
·
TOX analyzers ·
Organic Halides ·
Preview of Ion
Chromatography ·
Other Analyzers
(S, N) |
|
S: chapt
16C, 24D H: 16-6, 17-4 |
Prof El Sayess |
||
24 Sept |
Tu |
|
Prof
Wittbold |
||||
25 Sept |
W |
|
|
·
Detectors ·
Optical Systems B. Atomic Spec.
|
S: pp.312-325; 131-134, 143-189, 192-203, 206-227 H:Chapt.
21 |
|
|
6 Oct |
M |
·
Line sources ·
Sample
preparation |
|
S: Chapt.8&9 H:Chapt.
22 |
Lecture instead of lab |
||
|
|
·
Errors &
Interferences ·
Plasma
Instruments |
Lab1 due
on 3rd |
S: Chapt.8&9 H:Chapt.
22 |
|
||
7 Oct |
Tu |
C. Infrared Spec.·
FTIR ·
NDIR III. Specialized Analyzers·
Basics ·
Organic Carbon
& fractionation |
S: chapt
16C, 24D H: 16-6, 17-4 |
|
|||
9 Oct |
Th |
|
No Class – Feng Lecture |
|
|||
13 Oct |
M |
|
|
|
|||
14 Oct |
Tu |
IV. Sample Preparation·
Basics, LLE |
|
H:Chapt.23, 28 |
Monday
sched |
||
16 Oct |
Th |
·
Sample
extraction, fractionation |
|
H:Chapt.23, 28 |
|
||
20 Oct |
M |
|
Prof. Yu |
||||
21 Oct |
Tu |
·
Derivatization, clean-up |
|
H: Chapt
28 |
|
||
23 Oct |
Th |
V. Gas Chromatography·
Intro to
chromatography ·
System Basics |
|
S: Chapt.
26 H: Chapt.
23 |
|
||
27 Oct |
M |
·
Chromatographic
theory |
|
S: Chapt.
26 H: Chapt.
23 |
|
||
28 Oct |
Tu |
·
GC Detectors |
|
S: Chapt.
27 H: Chapt.
24 |
Prof. Yu |
||
30 Oct |
Th |
·
Inlet Systems ·
GC Columns and
stationary phases ·
Applications |
|
S: Chapt.
26 H: Chapt.
23 |
Prof. Yu |
||
3 Nov |
M |
·
Basics of Ion
Chromatography ·
Components of
an IC |
|
|
Xian |
||
4 Nov |
Tu |
VI. Liquid Chromatography·
LC Solvent
Selection ·
LC Detectors ·
Environmental
Applications |
|
S: H: Chapt.
23 |
|
||
6 Nov |
Th |
VII. Mass Spectrometry·
Basics ·
Detector for GC |
|
S: H: Chapt.
23 |
|
||
10 Nov |
M |
|
Xian |
||||
10 Nov |
M |
·
Interpretation
of Mass spectra |
|
S: H: Chapt.
28 |
|
||
11 Nov |
Tu |
|
HOLIDAY (Veteran’s Day) |
|
|||
12 Nov |
W |
|
No Class |
Tuesday class schedule |
|||
13 Nov |
Th |
|
Mid-term EXAM (2:30 PM) |
Through L#16 |
|||
18 Nov |
Tu |
·
MS
Instrumentation ·
MS Ionization |
|
|
Prof Yu |
||
20 Nov |
Th |
·
MS methods
continued |
|
|
. |
||
20 Nov |
Th |
|
Dutra |
||||
20 Nov |
Th |
|
Andreeva |
||||
24 Nov |
M |
|
Mahajan |
||||
24 Nov |
M |
|
Bliss |
||||
25 Nov |
Tu |
·
Chemical
Ionization |
|
|
|
||
Thanksgiving Recess |
|||||||
1 Dec |
M |
|
Mohan |
||||
1 Dec |
M |
|
Gao |
||||
2 Dec |
Tu |
·
Problems in
Analytical Analysis |
|
|
|
||
4 Dec |
Th |
·
Chromatographic
retention time and environmental properties |
|
|
|
Final Exam: Thursday, December 11, 2014 from 3:30-5:30 in Marston 211