CEE 772

Fall 2014

Detailed Schedule[1]

 

Click on L# to see full Overheads or P# to see printable version (2 slides/pg)

Date

Day

L#

P#

Lecture

Assignments

Reading[2]

Notes

2 Sept

Tu

1

1

I. Introduction

·         Course overview, administration, chemistry review

review assigned

S:pp.1-11

H:Chapt. 0

 

4 Sept

Th

2

2

·         Basics of Instrumental Analysis

·         Statistics

 

S: pp.11-18

H: Chapt 1-4

 

8 Sept

M

 
LAB #1a:UV/Vis Spectrophotometry
DAR

8 Sept

M

3

3

·         Detection Limits

II. Spectroscopy

·         Electron Transitions

·         Beer-Lambert’s Law

 

S: pp.116-120, 134-140, 300-312

H:Chapt. 1

Class instead of lab today

9 Sept

Tu

 
No Class – DAR Travel Day
 

11 Sept

Th

 
No Class – DAR Travel Day
 

15 Sept

M

 
LAB #1b:UV/Vis Spectrophotometry
DAR

16 Sept

Tu

4

4

A. Molecular Spec.

·         UV-Vis

·         Properties of spectrophotometers

·         Wavelength selectors

Lab1 assigned

S: Chapt. 14

H:Chapt. 19

Class instead of lab today

18 Sept

Th

 
No Class – DAR Travel Day
 

22 Sept

M

 

LAB #2: Atomic Abs. Spectrophotometry

ISB Chem lab

23 Sept

Tu

9

9

·         TOX analyzers

·         Organic Halides

·         Preview of Ion Chromatography

·         Other Analyzers (S, N)

 

S: chapt 16C, 24D

H: 16-6, 17-4

Prof El Sayess

29 Sept

M

 

LAB #3: Organic Carbon/ Nitrogen Analysis

Prof Wittbold

30 Sept

Tu

5

5

·         Detectors

·         Optical Systems

B. Atomic Spec.

  • Fundamentals

review presentation

S: pp.312-325; 131-134, 143-189, 192-203, 206-227

H:Chapt. 21

 

6 Oct

M

6

6

·         Line sources

·         Sample preparation

 

S: Chapt.8&9

H:Chapt. 22

Lecture instead of lab

 

 

7

7

·         Errors & Interferences

·         Plasma Instruments

Lab1 due on 3rd

 

S: Chapt.8&9

H:Chapt. 22

 

7 Oct

Tu

8

8

C. Infrared Spec.

·         FTIR

·         NDIR

III. Specialized Analyzers

·       Basics

·       Organic Carbon & fractionation

review due

S: chapt 16C, 24D

H: 16-6, 17-4

 

9 Oct

Th

 
No Class – Feng Lecture
 

13 Oct

M

 

HOLIDAY (Columbus Day)

 

14 Oct

Tu

10

10

IV. Sample Preparation

·         Basics, LLE

 

H:Chapt.23, 28

Monday sched

16 Oct

Th

11

11

·         Sample extraction, fractionation

 

H:Chapt.23, 28

 

20 Oct

M

 

LAB #4: Sample Preparation for GC/LC

Prof. Yu

21 Oct

Tu

12

12

·         Derivatization, clean-up

 

H: Chapt 28

 

23 Oct

Th

13

13

V. Gas Chromatography

·         Intro to chromatography

·         System Basics

 

S: Chapt. 26

H: Chapt. 23

 

27 Oct

M

14

14

·         Chromatographic theory

 

S: Chapt. 26

H: Chapt. 23

 

28 Oct

Tu

15

15

·         GC Detectors

 

S: Chapt. 27

H: Chapt. 24

Prof. Yu

30 Oct

Th

16

16

·         Inlet Systems

·         GC Columns and stationary phases

·         Applications

 

S: Chapt. 26

H: Chapt. 23

Prof. Yu

3 Nov

M

17

17

·         Basics of Ion Chromatography

·         Components of an IC

 

 

Xian

4 Nov

Tu

18

18

VI. Liquid Chromatography

·         LC Solvent Selection

·         LC Detectors

·         Environmental Applications

 

S:

H: Chapt. 23

 

6 Nov

Th

19

19

VII. Mass Spectrometry

·         Basics

·         Detector for GC

 

S:

H: Chapt. 23

 

10 Nov

M

 

LAB #5: TOX and IC

Xian

10 Nov

M

19

19

·         Interpretation of Mass spectra

 

S:

H: Chapt. 28

 

11 Nov

Tu

 

HOLIDAY (Veteran’s Day)

 

12 Nov

W

 

No Class

Tuesday class schedule

13 Nov

Th

 

Mid-term EXAM  (2:30 PM)

Through L#16

18 Nov

Tu

20

20

·         MS Instrumentation

·         MS Ionization

 

 

Prof Yu

20 Nov

Th

21

21

·         MS methods continued

 

 

.

20 Nov

Th

 

LAB #6: Gas Chromatography

Dutra

20 Nov

Th

 

LAB #7: High Performance Liquid Chromatography (PDA)

Andreeva

24 Nov

M

 

LAB #8: ICP/MS

Mahajan

24 Nov

M

 

LAB #9: LC/MS

Bliss

25 Nov

Tu

22

22

·         Chemical Ionization

 

 

 

Thanksgiving Recess

1 Dec

M

 

LAB #10: High Performance Liquid Chromatography (DLS)

Mohan

1 Dec

M

 

LAB #11: GC/MS

Gao

2 Dec

Tu

23

23

·         Problems in Analytical Analysis

 

 

 

4 Dec

Th

24

24

·         Chromatographic retention time and environmental properties

 

 

 

 

 

Final Exam:  Thursday, December 11, 2014 from 3:30-5:30 in Marston 211

 



[1] Tentative, subject to change

[2] S: refers to Skoog et al., H: refers to Harris.