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CEE 772 |
Fall 2005 |
Click on Lecture Number to see Lecture Overheads
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Date |
Day |
# |
Lecture |
Assignments |
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Notes |
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7 Sept |
W |
I. Introduction·
Course overview, administration, chemistry review
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S:pp.1-11 H:Chapt. 0 |
Gladys lectures |
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12 Sept |
M |
·
Basics of Instrumental Analysis
· Statistics |
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S: pp.11-18 H: Chapt 1-4 |
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13 Sept |
Tu |
LAB
#1:UV/Vis Spectrophotometry
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DAR
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14 Sept |
W |
·
Detection
Limits II. Spectroscopy·
Electron
Transitions ·
Beer-Lambert’s
Law |
S: pp.116-120, 134-140,
300-312 H:Chapt. 1 |
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19 Sept |
M |
A. Molecular Spec.·
UV-Vis ·
Properties of
spectrophotometers ·
Wavelength
selectors |
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S: Chapt. 14 H:Chapt. 19 |
Gladys lectures |
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20 Sept |
Tu |
Tyson
lab |
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21 Sept |
W |
·
Detectors ·
Optical Systems B. Atomic Spec.
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S: pp.312-325; 131-134, 143-189, 192-203,
206-227 H:Chapt. 21 |
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26 Sept |
M |
·
Line sources ·
Sample
preparation |
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S: Chapt.8&9 H:Chapt. 22 |
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27 Sept |
Tu |
Biochem lab |
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28 Sept |
W |
·
Errors &
Interferences ·
Plasma
Instruments |
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S: Chapt.8&9 H:Chapt. 22 |
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3 Oct |
M |
C. Infrared Spec.·
FTIR ·
NDIR III. Specialized Analyzers·
Basics ·
Organic Carbon
& fractionation |
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S: chapt 16C, 24D H: 16-6, 17-4 |
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4 Oct |
Tu |
Gladys |
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5 Oct |
W |
·
Organic Halides ·
Preview of Ion
Chromatography ·
Other Analyzers
(S, N) |
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S: chapt 16C, 24D H: 16-6, 17-4 |
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10 Oct |
M |
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11 Oct |
Tu |
Guanghui |
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12 Oct |
W |
IV. Sample Preparation·
Basics, LLE |
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H:Chapt.23, 28 |
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17 Oct |
M |
·
Sample
extraction, fractionation |
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H:Chapt.23, 28 |
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18 Oct |
Tu |
Gladys
& DAR |
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19 Oct |
W |
·
Derivatization,
clean-up |
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H: Chapt 28 |
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24 Oct |
M |
V. Gas Chromatography·
Theory ·
System Basics |
S: Chapt. 26 H: Chapt. 23 |
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25 Oct |
Tu |
Pesticide
Lab |
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26 Oct |
W |
·
System Basics ·
Detectors |
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S: Chapt. 27 H: Chapt. 24 |
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31 Oct |
M |
·
Theory |
S: Chapt. 26 H: Chapt. 23 |
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1 Nov |
Tu |
·
Inlet Systems ·
GC Columns and
stationary phases ·
Applications |
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S: H: Chapt. 23 |
Makeup for 7 Nov |
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2 Nov |
W |
VI. Mass Spectrometry·
Basics ·
Detector for GC |
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S: H: Chapt. 23 |
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4 Nov |
F |
·
Interpretation
of Mass spectra |
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S: H: Chapt. 28 |
Makeup for 8 Nov |
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7 Nov |
M |
No Class |
WQTC |
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8 Nov |
Tu |
No Lab |
WQTC |
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9 Nov |
W |
VII. Liquid Chromatography·
LC Solvent
Selection ·
LC Detectors ·
Environmental
Applications |
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14 Nov |
M |
·
Applications to
pesticides ·
Applications to
PAHs |
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Heymann/Huang |
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15 Nov |
Tu |
Heymann/Huang |
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16 Nov |
W |
First EXAM (11:15 in LGRC classroom) |
Through L#18 |
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18 Nov |
F |
·
Ion
Chromatographic systems ·
Ion Suppression |
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S: H: |
Hua lecture; Makeup for 14
Nov |
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21 Nov |
M |
VI. Mass Spectrometry·
ICP/MS
applications |
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Goodwell/Mercer |
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22 Nov |
Tu |
Goodwell/Mercer |
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23 Nov |
W |
·
Fragmentation
and MS interpretation ·
EI vs CI |
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28 Nov |
M |
·
Applications to
Perchlorate and Mn complexes |
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Sahu/
Islam |
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29 Nov |
Tu |
Sahu/
Islam |
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30 Nov |
W |
·
High resolution
MS ·
Magnetic
Sectors |
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5 Dec |
M |
·
Applications to
nitrosamines |
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Briggs/
Liu |
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6 Dec |
Tu |
Briggs/
Liu |
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7 Dec |
W |
·
Ion Traps, TOF |
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12 Dec |
M |
·
Electrospray,
APCI |
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S: H: C |
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13 Dec |
Tu |
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14 Dec |
W |
·
Endocrine
disruptors |
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Final Exam: Friday Dec 16th at 8AM in Marston 220